Reaktion #1946550

ord-8bcbfa809426476db72b76e486fe6dd5

Reaktionsgleichung

CCCCCCCC(=O)N(C)CCC(=O)O
N-octanoyl-N-methyl-β-alanine
CC(C)O
isopropanol
O=S(=O)(O)O
sulfuric acid
→
CCCCCCCC(=O)N(C)CCC(=O)OC(C)C
N-octanoyl-N-methyl-β-alanine isopropyl ester

Edukte

CCCCCCCC(=O)N(C)CCC(=O)O
N-octanoyl-N-methyl-β-alanine
CC(C)O
isopropanol
O=S(=O)(O)O
sulfuric acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    TemperaturThe mixture was heated
  2. 2
    Temperaturunder reflux
  3. 3
    Sonstigereaction for 8 hours

Vorschrift

Fifty-seven(57) grams of N-octanoyl-N-methyl-β-alanine and 500 ml of isopropanol were charged into a 1,000-milliliter flask, and 1 ml of conc. sulfuric acid was further added thereto as the catalyst. The mixture was heated under reflux reaction for 8 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06528068B1uspto-grants-2003_03