Reaktion #1928056

ord-f154095bac52406cbf0e4a501587cc29

Reaktionsgleichung

CCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
Intermediate 6a
CCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
N-Hexyl-6-acetyl-4,4-dimethyl-3,4-dihydro-1H-quinolin-2-one
CCCCCCCI
1-iodo-n-heptane
→
CCCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
title compound
CCCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
N-Heptyl-6-acetyl-4,4-dimethyl-3,4-dihydro-1H-quinolin-2-one

Edukte

CCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
Intermediate 6a
CCCCCCN1C(=O)CC(C)(C)c2cc(C(C)=O)ccc21
N-Hexyl-6-acetyl-4,4-dimethyl-3,4-dihydro-1H-quinolin-2-one
CCCCCCCI
1-iodo-n-heptane

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Following a procedure similar to that used for the preparation of Intermediate 6a but using 1-iodo-n-heptane as the alkylating reagent the title compound was obtained as a colorless oil (66% yield).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06683092B1uspto-grants-2004_01