Reaktion #1918294

ord-50556b17064046d383d6cb97e1040bfa

Reaktionsgleichung

Cc1c(Cc2c(F)cccc2Cl)c(=O)oc2cc(O)ccc12
3-(2-chloro-6-fluoro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide
→
Cc1c(Cc2c(F)cccc2Cl)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
title compound
Cc1c(Cc2c(F)cccc2Cl)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
Methyl-phenyl-carbamic acid 3-(2-chloro-6-fluoro-benzyl)-4-methyl-2-oxo-2H-chromen-7-yl ester

Edukte

Cc1c(Cc2c(F)cccc2Cl)c(=O)oc2cc(O)ccc12
3-(2-chloro-6-fluoro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 3-(2-chloro-6-fluoro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide by applying procedure 3. HPLC-MS m/z=452 (M+1), Rt: 5.15 min.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07067517B2uspto-grants-2006_06