Reaktion #1918293

ord-1933850d9ef14c9b9d937fde33a97819

Reaktionsgleichung

Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(O)ccc12
3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide
→
Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
title compound
Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
Methyl-phenyl-carbamic acid 3-(3,4-dichloro-benzyl)-4-methyl-2-oxo-2H-chromen-7-yl ester

Edukte

Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(O)ccc12
3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide (white solid). HPLC-MS m/z=468 (M+1), Rt: 5.47 min.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07067517B2uspto-grants-2006_06