Reaktion #1918292

ord-e1213a0b3a63499297829e44384c0038

Reaktionsgleichung

Cc1c(Cc2ccccc2)c(=O)oc2cc(O)ccc12
3-benzyl-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide
→
Cc1c(Cc2ccccc2)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
title compound
Cc1c(Cc2ccccc2)c(=O)oc2cc(OC(=O)N(C)c3ccccc3)ccc12
Methyl-phenyl-carbamic acid 3-(benzyl)-4-methyl-2-oxo-2H-chromen-7-yl ester

Edukte

Cc1c(Cc2ccccc2)c(=O)oc2cc(O)ccc12
3-benzyl-7-hydroxy-4-methyl-2H-chromen-2-one
CN(C(=O)n1cc[n+](C)c1)c1ccccc1.[I-]
3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 3-benzyl-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide. HPLC-MS m/z=400 (M+1), Rt: 4.90 min.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07067517B2uspto-grants-2006_06