Reaktion #1914811

Reaktionsgleichung

3-methyl-1,4-benzoquinone-4-oxime

acetic anhydride

→

3-methyl-1,4-benzoquinone-4-(O-acetyloxime)

Lösungsmittel

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAt the end of the reaction
2. 2
   FiltrationThe precipitated product was filtered off
3. 3
   Waschenwashed with water
4. 4
   Sonstigedried

Vorschrift

One drop of pyridine was added to a mixture of 0.5 g (3.6 mmol) of 3-methyl-1,4-benzoquinone-4-oxime and 1 mL of acetic anhydride and the resulting mixture was heated to 70° C. At the end of the reaction, the reaction mixture was poured on 10 mL of water/ice. The precipitated product was filtered off, washed with water and then dried.

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