Reaktion #1904039

Reaktionsgleichung

hydroxy amine

glutaric anhydride

→

Hydroxylamine Glutarate

Lösungsmittel

benzene

triethyl amine

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturrefluxed for 2 h
2. 2
   SonstigeThe solvent is evaporated under vacuum
3. 3
   Sonstigethe residue is purified by flash chromatography

Vorschrift

This example that demonstrates how this method could be performed. Part 1: To a solution of 2 g hydroxy amine in 100 ml dry benzene and 20 ml triethyl amine, 9.4 g glutaric anhydride is added and the reaction mixture stirred at room temperature for 2 h and refluxed for 2 h. The solvent is evaporated under vacuum and the residue is purified by flash chromatography using silica gel.

Quelle