Reaktion #1885010

Reaktionsgleichung

styrene

butyl acrylate

acrylic acid

dodecanethiol

sodium dodecylbenzenesulfonate

→

Styrene Butyl Acrylate Acrylic Acid

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeIn a reactor equipped with a reflux condenser, a stirrer
2. 2
   workup.ADDITIONa nitrogen-introducing pipe

Vorschrift

In a reactor equipped with a reflux condenser, a stirrer, a nitrogen-introducing pipe, and a monomer dripping funnel, 3.3 parts of sodium dodecylbenzenesulfonate is dissolved in 3,824 parts of ion exchange water. Subsequently, 30.6 parts of styrene, 9.4 parts of butyl acrylate, 1.2 parts of acrylic acid dimer, and 0.3 parts of dodecanethiol are added thereto, and thoroughly stirred at room temperature for emulsification stabilization (emulsified liquid 1).

Quelle