Reaktion #1880949
ord-e3da1ad9914a4f978033cb83e4daf5c9
Reaktionsgleichung
Cyclohexylethyl alcohol
ethyl vinyl ether
→
cyclohexylethyl vinyl ether
Reagenzien
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThe resultant reaction mixture
- 2Extraktionwas extracted with ethyl acetate and water
- 3Waschenthe extract was washed with water
- 4workup.DISTILLATIONdistilled under reduced pressure
Vorschrift
Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.