Reaktion #1869202

Reaktionsgleichung

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate

chloroform

→

product

Ausbeute 100.0%

1-[2-(4-quinolinyl)ethyl]-4-piperidinamine trihydrochloride

Ausbeute 100.0%

Lösungsmittel

HCl

dioxane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe reaction mixture was evaporated to dryness

Vorschrift

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate (9a) (278 mg) was dissolved in chloroform and diluted with 4N HCl in dioxane solution. After stirring two hours, the reaction mixture was evaporated to dryness to afford the product as a solid (180 mg, 100%).

Quelle