Reaktion #1858595

ord-ceaa6c2a00dd4123ab46110c52170bf6

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigethe procedure of synthesis method C and separation methods F and G

Vorschrift

The title compound was prepared from 2-(5-bromoisochroman-1-yl)-4,5-dihydro-1H-imidazole (50 mg) and (tributylstannyl)methanol (86 mg) by using tetrakis(triphenyl-phosphine)palladium (10.28 mg) as catalyst, and the procedure of synthesis method C and separation methods F and G. (Yield 6.2 mg).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09249127B2uspto-grants-2016_02