Reaktion #1850940

Reaktionsgleichung

N-p-chlorobezenesulfonyl-sarcosine

diazomethane

→

N-p-chlorobenzenesulfonyl-sarcosine methyl ester

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe precipitated reaction product
2. 2
   Filtrationis collected by filtration

Vorschrift

2 Parts of N-p-chlorobezenesulfonyl-sarcosine is added to a diazomethane-ethereal solution. After the generation of nitrogen has ceased, the precipitated reaction product is collected by filtration to obtain 1.2 parts of N-p-chlorobenzenesulfonyl-sarcosine methyl ester, m.p. 80°-80.5° C.

Quelle