Reaktion #1848747

Reaktionsgleichung

acid 12

3-[5-(4-Chlorophenyl)-1-(4-methoxyphenyl)-3-pyrazolyl]propionic acid

NaOH

→

13

Ausbeute 98.0%

Sodium 3-[5-(4-chlorophenyl)-1-(4-methoxyphenyl)-3-pyrazolyl]propanoate monohydrate

Ausbeute 98.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISTILLATIONdistilled H2O (15 ml)

Vorschrift

To the acid 12 (1.0169 g, 2.85 mM) was added a 1.00N NaOH solution (2.85 ml, 2.85 mM) and distilled H2O (15 ml). The reaction mixture was stirred until it was homogeneous, and then lyophilized to afford 13 (1.08 g, 98%) as a white solid, with a mp greater than 300° C.

Quelle