Reaktion #1817657

Reaktionsgleichung

methyl chloride

4-chlorobenzaldehyde thiosemicarbazone

→

title compound

Methyl 3-(4-chlorobenzylidene)thiocarbazimidate hydrochloride

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturheated in an oil bath for 11/2 hour

Vorschrift

A 10% molar excess of methyl chloride is added to 2.14 g. of 4-chlorobenzaldehyde thiosemicarbazone and 25 ml. of a anhydrous ethanol in a pressure vessel. The reaction mixture is magnetically stirred and heated in an oil bath for 11/2 hour. The crystalline title compound separates on cooling and is filtered off and air dried.

Quelle