Reaktion #1797957

Reaktionsgleichung

4-(3-chloropropoxy)-2-fluorobenzoyl chloride

ammonia

→

4-(3-chloropropoxy)-2-fluorobenzamide

Ausbeute 61.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe mixture is then filtered

Vorschrift

4-(3-chloropropoxy)-2-fluorobenzoyl chloride i80 (0.73 g, 2.91 mmol, 1 eq) is treated with aqueous ammonia (35 ml) and the resulting mixture is vigorously stirred at room temperature overnight. The mixture is then filtered to give 0.41 g of 4-(3-chloropropoxy)-2-fluorobenzamide i82 as a white solid.

Quelle