Reaktion #1780293

Reaktionsgleichung

4-bromo-2-ethylaniline

5-fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride

→

desired compound

Ausbeute 46.6%

5-Fluoro-3-methyl-benzo[b]thiophene-2-sulfonic acid(4-bromo-2-ethyl-phenyl)-amide

Ausbeute 46.6%

Lösungsmittel

pyridine

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound was prepared in analogy to Example 1

Vorschrift

This compound was prepared in analogy to Example 1, starting from 4-bromo-2-ethylaniline (CAS:45762-41-2, 2.0 g) and 5-fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride (0.265 g) in pyridine (2.0 ml) for 4 h to obtain the desired compound (0.20 g) as a colorless solid. MS (ISP): 445.0, 447.0 (M+NH4)+

Quelle