Reaktion #1764048

ord-a66f4eef52e24031ace738ed12e4250e

Reaktionsgleichung

CCN(C)CC
diethylmethylamine
Cc1ccc(S(=O)(=O)O)cc1.O
p-toluenesulfonic acid monohydrate
→
CCN(C)CC
diethylmethylamine
Cc1ccc(S(=O)(=O)O)cc1
p-toluenesulfonic acid

Edukte

CCN(C)CC
diethylmethylamine
Cc1ccc(S(=O)(=O)O)cc1.O
p-toluenesulfonic acid monohydrate

Reagenzien

Keine

Lösungsmittel

CCC(C)=O
2-butanone

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.DISTILLATIONthe solvent was then distilled off in vacuo
  2. 2
    SonstigeThe obtained solid was recrystallized from acetone

Vorschrift

3.0 g of diethylmethylamine was dissolved in 30 cm3 of 2-butanone, to which was then gradually added 5.7 g of p-toluenesulfonic acid monohydrate while stirring. The stirring was continued for an additional one hour, and the solvent was then distilled off in vacuo. The obtained solid was recrystallized from acetone to obtain a diethylmethylamine salt of p-toluenesulfonic acid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08007878B2uspto-grants-2011_08