Reaktion #1752014

Reaktionsgleichung

2-Amino-4,4,4-trifluorobutanoic acid

HCl

ethanol

→

1-Ethoxy-4,4,4-trifluoro-1-oxobutan-2-aminium chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturto cool to ambient temperature
2. 2
   Einengenconcentrated

Vorschrift

2-Amino-4,4,4-trifluorobutanoic acid (11.7 g, 52.8 mmol) was added to a saturated solution of HCl in ethanol (100 mL) and heated to 85° C. After 4 h, the mixture was allowed to cool to ambient temperature and concentrated. MS 186.0 (M+1).

Quelle