Reaktion #1723511

ord-374d5ae4a94441e3a3f31b5784d5f55c

Reaktionsgleichung

CCCC[C@H](NC(=O)[C@H](C)NC(=O)[C@@H](NC(=O)c1ccccc1)C(C)C)C(=O)O.O=C(CBr)CBr
N-benzoyl-L-valyl-L-alanyl-L-norleucine bromomethyl ketone
O=C(O)c1c(F)c(F)c(F)c(F)c1F
2,3,4,5,6-pentafluorobenzoic acid
→
CC(=O)OC(=O)c1c(F)c(F)c(F)c(F)c1F.CCCC[C@H](NC(=O)[C@H](C)NC(=O)[C@@H](NC(=O)c1ccccc1)C(C)C)C(=O)O
N-Benzoyl-L-valyl-L-alanyl-L-norleucine 2,3,4,5,6-pentafluoro benzoyloxy methyl ketone

Edukte

CCCC[C@H](NC(=O)[C@H](C)NC(=O)[C@@H](NC(=O)c1ccccc1)C(C)C)C(=O)O.O=C(CBr)CBr
N-benzoyl-L-valyl-L-alanyl-L-norleucine bromomethyl ketone
O=C(O)c1c(F)c(F)c(F)c(F)c1F
2,3,4,5,6-pentafluorobenzoic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

(Electrospray MS m/z 614 [MH+ ]) from of N-benzoyl-L-valyl-L-alanyl-L-norleucine bromomethyl ketone and 2,3,4,5,6-pentafluorobenzoic acid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06034066uspto-grants-2000_03