Reaktion #172101

Reaktionsgleichung

tert-butyl 1-carbamoylcyclopentylcarbamate

HCl

HCl

→

1-aminocyclopentanecarboxamide hydrochloride

Lösungsmittel

dioxane

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenIt was then concentrated in vacuo

Vorschrift

A solution of tert-butyl 1-carbamoylcyclopentylcarbamate (305 mg, 1.33 mmol) in 4N HCl in dioxane (5 mL) and aq. 6N HCl (3 mL) was stirred at room temperature for 3 h. It was then concentrated in vacuo to give 1-aminocyclopentanecarboxamide hydrochloride as a solid (214 mg).

Quelle