Reaktion #171139

Reaktionsgleichung

α-methylene-γ-valerolactone

benzene

divinyl benzene

→

α-methylene-γ-valerolactone divinyl benzene

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeTo a dry 100 mL round bottom flask equipped with a magnetic stir bar
2. 2
   SonstigeThe reactor was purged with nitrogen for 30 minutes
3. 3
   Temperaturbefore letting cooling the reaction mixture to room temperature
4. 4
   Sonstigedrying under vacuum

Vorschrift

To a dry 100 mL round bottom flask equipped with a magnetic stir bar was charged 1.0153 g (8.98×10−3 mol) α-methylene-γ-valerolactone, 16.78 g (0.215 mol) benzene, 0.0561 g (4.31×10−4 mol) divinyl benzene, and 0.0067 g (4.08×10−5 mol) azobisisobutylnitrile. The reactor was purged with nitrogen for 30 minutes before heating to 65° C. The reactor was held at 65° C. for 5 hours before letting cooling the reaction mixture to room temperature and drying under vacuum.

Quelle