Reaktion #1708380

ord-d9fd6f8899674acb8d20ae54423b0202

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeSlowly add hydrochloric acid, and white precipitation
  2. 2
    workup.STIRRINGStir the slurry for at least 4 hours
  3. 3
    Filtrationfilter the slurry

Vorschrift

In a large beaker, add naphthionic acid sodium salt and water and stir to complete solution, pH=9.2-9.4. Slowly add hydrochloric acid, and white precipitation occurs at pH=2.2-2.4. Stir the slurry for at least 4 hours, then filter the slurry. Use the wetcake in Stage 2.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08772545B2uspto-grants-2014_07