Reaktion #170319

ord-d0554a735d3f4edb8b58bab4db52ce4d

Reaktionsgleichung

Cc1onc(-c2ccccc2)c1COc1ccc(C(=O)O)cn1
6-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-nicotinic acid
NC1CCC1
cyclobutylamine
Cc1onc(-c2ccccc2)c1COc1ccc(C(=O)NC2CCC2)cn1
title compound
Ausbeute 56.0%
Cc1onc(-c2ccccc2)c1COc1ccc(C(=O)NC2CCC2)cn1
N-Cyclobutyl-6-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-nicotinamide
Ausbeute 56.0%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

As described for example 8b, 6-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-nicotinic acid (100 mg, 0.32 mmol) was converted, using cyclobutylamine (1 M in DMF) instead of methylamine, to the title compound (66 mg, 56%) which was obtained as a white solid. MS: m/e=364.4 [M+H]+.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08846719B2uspto-grants-2014_09