Reaktion #1702337
ord-5969ccb1707f45ba95fc44edb647bb70
Reaktionsgleichung
(9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde
(S)-1-phenyl-propylamine
→
title compound
Ausbeute 50.0%
3,3-Dimethyl-9-{2-[(S)-1-phenyl-propylamino]-ethyl}-1,5-dioxa-spiro[5.5]undecan-9-ol
Ausbeute 50.0%
Edukte
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-phenyl-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 50% of theory; LC (method 8): tR=1.16 min; Mass spectrum (ESI+): m/z=362 [M+H]+.