Reaktion #1701205

ord-5fa88220f76b4466b95e15b1fb8bf209

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

First, one mole of ethanolamine is reacted with each mole of 3,3'-dimethoxy-2,2',4,4',6,6'-hexanitrobiphenyl under the conditions given in example 6 to give 3-methoxy-3'-(2-hydroxyethylamino)-2,2',4,4',6,6'-hexanitrobiphenyl (compound X). Compound X is then reacted with ammonia under the conditions of example 7 to produce 3-amino-3'-(2-hydroxyethylamino)-2,2',4,4',6,6'-hexanitrobiphenyl (compound XI). Compound XI is then nitrated under the conditions of example 8 to produce the product 3-amino-3'-(hydroxyethylaminonitrate)-2,2',4,4',6,6'-hexanitrobiphenyl.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05194659uspto-grants-1993_03