Reaktion #1681361

Reaktionsgleichung

sodium bicarbonate

triethylamine

methanesulfonyl chloride

3-{[tert-butyl(dimethyl)silyl]oxy}-2,2-dimethylpropan-1-ol

→

tert-butyl(3-ethoxy-2,2-dimethylpropoxy)dimethylsilane

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe reaction liquid
2. 2
   Sonstigeto the reaction liquid

Vorschrift

To a solution of 3-{[tert-butyl(dimethyl)silyl]oxy}-2,2-dimethylpropan-1-ol (Registry No. 117932-70-4) (2.18 g, 10 mmol) in THF (30 ml) were added triethylamine (1.67 ml, 12 mmol) and methanesulfonyl chloride (0.85 ml, 11 mmol) under ice cooling. The reaction liquid was stirred at room temperature for 30 minutes, and to the reaction liquid was added an aqueous solution of sodium bicarbonate.

Quelle