Reaktion #167608

Reaktionsgleichung

product

4-(5-Bromopyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

phenylboronic acid

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title compound

4-(5-phenylpyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

Reaktionsbedingungen

Vorschrift

The title compound was prepared from the product of Example 65A and phenylboronic acid according to General Method B: 1H NMR (500 MHz, CDCl3) δ ppm 6 ppm 8.14 (d, 2 H), 7.56 (d, 2 H), 7.46 (t, 2 H), 7.39 (t, 1 H), 7.10 (s, 1 H), 3.73-3.37 (m, 5 H), 3.05-2.97 (m, 3 H), 2.27-2.17 (m, 4 H), 1.88-1.77 (m, 3 H); LC-MS Method D (ESI+) m/z 306.0 (M+H)+, retention time 1.28 minutes.

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