Reaktion #1674927

Reaktionsgleichung

1-diethoxymethyl-2-nitroiminoimidazolidine

o-aminobenzonitrile

DMF

→

1-(2-cyanophenyliminomethyl)-2-nitroiminoimidazolidine

Ausbeute 85.4%

Lösungsmittel

Ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationthe resultant crystals were collected by filtration
2. 2
   Sonstigedried

Vorschrift

0.05 g of boron trifluoride ether complex was added to a mixture of 2.0 g of 1-diethoxymethyl-2-nitroiminoimidazolidine, 1.02 g of o-aminobenzonitrile and 5 ml of DMF, followed by agitation at room temperature for 15 minutes. Ether was added to the reaction mixture, and the resultant crystals were collected by filtration and dried to give 1.9 g of 1-(2-cyanophenyliminomethyl)-2-nitroiminoimidazolidine.

Quelle