Reaktion #1663546

Reaktionsgleichung

di-t-butyl peroxide

β-bromo ethyl bromo benzene

methanol

→

bromostyrene

Ausbeute 95.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONThe mixture was added to the reactor in a manner
2. 2
   Temperaturheated to 300°-320°C
3. 3
   SonstigeThe products were collected as in Example 1

Vorschrift

2 g di-t-butyl peroxide were dissolved in 100 g β-bromo ethyl bromo benzene. The mixture was added to the reactor in a manner described in Example 1, together with 25 g methanol and nitrogen at a flow rate of 2 l/h. The reactor was a glass spiral made of a 6 mm wide 5 m long tube heated to 300°-320°C. The products were collected as in Example 1 and consisted of 58 g bromostyrene and 12 g unconverted reactant. The yield was 95% bromostyrene.

Quelle