Reaktion #1635

Reaktionsgleichung

n-hexylphosphinic acid, n-butyl ester

paraformaldehyde

→

title compound

n-Hexylhydroxymethylphosphinic acid, n-butyl ester

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigePurification by chromatography
2. 2
   Wascheneluting with dichloromethane containing 5% methanol
3. 3
   Sonstigegave an oil

Vorschrift

The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

Quelle