Reaktion #160951

ord-7960dd31f1db4e9b9ea4d410a00d6e98

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeto afford a white crystalline solid

Vorschrift

The title compound was prepared in an analogous fashion to that described in Stage 11.2 using 5-bromo-6-chloro-nicotinic acid and 4-pentafluoroethyl-aniline to afford a white crystalline solid. HPLC (Condition 4) tR=6.61 min, UPLC-MS (Condition 3) tR=1.32 min, m/z=429 [M−H]−.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08829195B2uspto-grants-2014_09