Reaktion #160596

Reaktionsgleichung

5,6-difluoro-N1-(2-fluoro-4-iodophenyl)benzene1,2-diamine

3-bromo-5-chlorothiophene-2-sulfonyl chloride

→

title compound

3-Bromo-5-chloro-N-(3,4-difluoro-2-(2-fluoro-4-iodophenylamino)phenyl)thiophene-2-sulfonamide

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeto obtain

Vorschrift

According to the general procedure B, 5,6-difluoro-N1-(2-fluoro-4-iodophenyl)benzene1,2-diamine was reacted with 3-bromo-5-chlorothiophene-2-sulfonyl chloride to obtain, the title compound. 1H NMR (300 MHz, CDCl3): δ 7.41 (dd, J=2.1 & 10.5 Hz, 1H), 7.35 (br m, 2H), 7.31 (dd, J=2.1 & 4.2 Hz, 1H), 7.19 (d, J=8.7 Hz, 1H), 7.08 (dd, J=9.0 & 17.4 Hz, 1H), 6.02(dt, J=2.1, 8.4 & 17.1 Hz, 1H), 5.59 (br s, 1H).

Quelle