Reaktion #1605792

ord-856333b9505d437b9cb299b1db0cbd23

Reaktionsgleichung

O.O.O.O.O.OC[C@H]1O[C@H](OC[C@H]2O[C@H](O[C@]3(CO)O[C@H](CO)[C@@H](O)[C@@H]3O)[C@H](O)[C@@H](O)[C@@H]2O)[C@H](O)[C@@H](O)[C@H]1O
Raffinose pentahydrate
O.O=C[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO
glucose monohydrate
→
OC[C@H]1O[C@H](OC[C@H]2O[C@H](O[C@]3(CO)O[C@H](CO)[C@@H](O)[C@@H]3O)[C@H](O)[C@@H](O)[C@@H]2O)[C@H](O)[C@@H](O)[C@H]1O
raffinose
Ausbeute 4.5%
O=C[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO
glucose

Edukte

O.O.O.O.O.OC[C@H]1O[C@H](OC[C@H]2O[C@H](O[C@]3(CO)O[C@H](CO)[C@@H](O)[C@@H]3O)[C@H](O)[C@@H](O)[C@@H]2O)[C@H](O)[C@@H](O)[C@H]1O
Raffinose pentahydrate
O.O=C[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO
glucose monohydrate

Reagenzien

Keine

Lösungsmittel

O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Raffinose pentahydrate or glucose monohydrate was dissolved in nano-pure water to obtain 4.5% (w/v) raffinose or glucose. To the solution, leucine was added and the pH was adjusted to 7.0. The concentration of the leucine in the solution ranged between 0.8% and 1.6% (w/v).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09072783B2uspto-grants-2015_07