Reaktion #159390

Reaktionsgleichung

1-(4-Nitro-phenyl)-[1,4]diazepane

Methansulfonyl-ethene

→

1-(2-Methanesulfonyl-ethyl)-4-(4-nitro-phenyl)-[1,4]diazepane

Lösungsmittel

Methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe volatiles were removed in vacuo
2. 2
   SonstigeThe product with the molecular weight of 327.40 (C14H21N3O4S) was obtained in this way

Vorschrift

A mixture of 1-(4-Nitro-phenyl)-[1,4]diazepane (4.90 g), Methansulfonyl-ethene (2.35 g) and Methanol (50 mL) was stirred for 2 h at room temperature. The volatiles were removed in vacuo. The product with the molecular weight of 327.40 (C14H21N3O4S) was obtained in this way; MS (ESI): 328 (M+H+).

Quelle