Reaktion #158230

ord-6183f732df1949c2a490b2e4ae7362c5

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigewas prepared
  2. 2
    Sonstigefor 10 hours

Vorschrift

A complex reducing agent was prepared by reacting sodium (0.034 g/4.86 mmol) and naphthalene (0.622/4.86 mmol) in 70 ml of tetrahydrofuran under Ar flow in a 250 ml 1-neck round flask for 10 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08822714B2uspto-grants-2014_09