Reaktion #157904

ord-81dc4ea8c152498aaf44befe36b0dc78

Reaktionsgleichung

OB(O)O.OB(O)O.OB(O)O.[Na+].[Na+].[O-]B([O-])O
disodium tetraborate
[Ti]
titanium
OO
H2O2
→
[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[Ti+4].[Ti+4].[Ti+4]
Titanium Borate

Edukte

OB(O)O.OB(O)O.OB(O)O.[Na+].[Na+].[O-]B([O-])O
disodium tetraborate
[Ti]
titanium
OO
H2O2

Reagenzien

Keine

Lösungsmittel

O
water
O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeis in the temperature range of about 85° C. to about 95° C
  2. 2
    Sonstigeto form a dark slurry
  3. 3
    Sonstigeresulted
  4. 4
    FiltrationThe product was filtered in a Büchner funnel
  5. 5
    Waschenthe cake was washed with deionized water
  6. 6
    Sonstigedrying

Vorschrift

200 g of disodium tetraborate was dissolved in 800 ml of hot deionized water. The water is in the temperature range of about 85° C. to about 95° C. 150 g of 45% titanium III sulfate was added to the above solution to form a dark slurry. 35% H2O2 was added drop-wise to the slurry until a homogenous yellow suspension resulted. The product was filtered in a Büchner funnel, and the cake was washed with deionized water. Solids were determined to be 19.8% by oven drying.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08822582B2uspto-grants-2014_09