Reaktion #157629

Reaktionsgleichung

3-bromopropanoyl chloride

diethylamine

→

3-Bromo-N,N-diethylpropanamide

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationthe resulting white solid was filtered
2. 2
   Einengenthe filtrate was concentrated
3. 3
   Sonstigeto give a crude oil which
4. 4
   Sonstigewas used in the next reaction without further purification

Vorschrift

A mixture of 3-bromopropanoyl chloride (1.0 g, 5.8 mmol) and diethylamine (1.9 g, 26 mmol) in THF (20 ml) was stirred at 0° C. for 30 min, the resulting white solid was filtered and the filtrate was concentrated to give a crude oil which was used in the next reaction without further purification.

Quelle