Reaktion #157567

Reaktionsgleichung

2-amino-4-chlorobenzenethiol

2-(chloromethyl)pyrimidine

K2CO3

→

title compound

Ausbeute 50.8%

5-chloro-2-((pyrimidin-2-ylmethyl)thio)aniline

Ausbeute 50.8%

Lösungsmittel

DMF

Reaktionsbedingungen

Vorschrift

Following General Procedure A, the title compound (284 mg, 39%) was prepared from 2-amino-4-chlorobenzenethiol (529 mg, 3.33 mmol), 2-(chloromethyl)pyrimidine (366 mg, 2.22 mmol) and K2CO3 (1.53 g, 11.09 mmol) in DMF (10 ml).

Quelle