Reaktion #1527484

ord-2f452d3bab23462a84f5f99d56ff15b2

Reaktionsgleichung

N[C@@H](CCO)C(=O)O
Homoserine
C[C@@H](O)[C@H](N)C(=O)O
threonine
CC[C@H](C)[C@H](N)C(=O)O
isoleucine
CC(C)[C@H](N)C(=O)O
valine
CN[C@@H]1[C@H](O)[C@H](NC)[C@H]2O[C@@]3(O)C(=O)C[C@@H](C)O[C@H]3O[C@@H]2[C@H]1O
spectinomycin
O=P([O-])([O-])O.[K+].[K+]
K2HPO4
O=S(=O)([O-])[O-].[Mg+2]
MgSO4
O=P([O-])(O)O.[K+]
KH2PO4
O=C([O-])[O-].[Ca+2]
CaCO3
OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O
lactose
O=C(O)CCCC[C@@H]1SC[C@@H]2NC(=O)N[C@@H]21
biotin
NCCCC[C@H](N)C(=O)O
L-lysine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONwere added to the production medium for ATCC 21086 strain and its transformant
  2. 2
    workup.WAITwas carried out at 30° C. for 72 hours

Vorschrift

Each strain was cultured in NB medium at 30° C. for 16 hours. For the culture of the transformants, spectinomycin was added to NB medium at a concentration of 100 μg/ml. Then, 0.5 ml of the seed culture was inoculated into 5 ml of a production medium (pH 7.2) comprising 100 g/l lactose, 30 g/l (NH4)2SO4, 0.5 g/l KH2PO4, 0.5 g/l K2HPO4, 1 g/l MgSO4 ·7H2O, 10 mg/l FeSO4 ·7H2O, 10 mg/l MnSO4 ·7H2O, 100 μg/l biotin and 30 g/l CaCO3 in a test tube. Homoserine (100 μg/ml) was further added to the production medium for RH6 strain and its transformant, and 100 μg/ml each of threonine, isoleucine and valine were added to the production medium for ATCC 21086 strain and its transformant. Shaking culture was carried out at 30° C. for 72 hours. After the culturing was finished, the amount of L-lysine formed was colorimetrically determined by the acidic copper ninhydrin method [Chinard, J. Biol. Chem., 199, 91 (1952)]. The results are shown in Table 7.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05498532uspto-grants-1996_03