Reaktion #1526130

Reaktionsgleichung

N-vinylpyrrolidone

vinyl laurate

→

N-Vinylpyrrolidone vinyl laurate

Lösungsmittel

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resulting reaction mixture
2. 2
   Sonstigeprecipitated
3. 3
   SonstigeAfter completion of the reaction
4. 4
   workup.DISTILLATIONthe methanol was distilled off
5. 5
   Waschenthe polymer was washed a few times with fresh methanol

Vorschrift

To a solution of 27.75 gm (0.25 mol) of N-vinylpyrrolidone and 169.5 gm (0.75 mol) of vinyl laurate in 460 gm of methanol were added 6 gm of azobisisobutyronitrile as catalyst. The resulting reaction mixture was agitated for 6 hours at 60° C, during which time the copolymer precipitated. After completion of the reaction, the methanol was distilled off and the polymer was washed a few times with fresh methanol. The yield was 176.5 gm (90% of theory) of N-vinylpyrrolidone/vinyl laurate copolymer (1:3 molar ratio).

Quelle