Reaktion #1516490

ord-6bf30d76f105458abf336a2d91aa06a1

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

To a stirred solution of monoethyl malonate 1(1.65 g, 12.5 mmol) in THF (25 mL) was added the magnesium ethoxide (0.61 g, 6.25 mmol). The reaction mixture was allowed to stir at rt for 5 h (until the solution become clear). The result solution was used for next step without any treatment.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08940506B2uspto-grants-2015_01