Reaktion #1492107

Reaktionsgleichung

2-(benzo[d]thiazol-2-ylthio)acetic acid

1,2,3,4-tetrahydrobenzo[b]azepin-5-one

1,2,3,4-tetrahydro-benzo[b]azepin-5-one

→

37

Ausbeute 29.0%

1-(2-(Benzo[d]thiazol-2-ylthio)acetyl)-1,2,3,4-tetrahydro-benzo[b]azepin-5-one

Ausbeute 29.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe title compound was synthesized

Vorschrift

The title compound was synthesized according to General Procedure B using 2-(benzo[d]thiazol-2-ylthio)acetic acid and 1,2,3,4-tetrahydrobenzo[b]azepin-5-one (5) to yield 37 (160 mg, 29%): MS (APCI): m/z 369 [M+H]+. Anal. Calcd. for C19H16N2O2S2: C, 61.93; H, 4.38; N, 7.60. Found: C, 61.72; H, 4.31; N, 7.40.

Quelle