Reaktion #1473036
ord-85de58f66ddc43c29b946c8b4aa54e18
Reaktionsgleichung
tetramethylammonium hydroxide
pentafluorobenzenesulfonyl chloride
→
tetramethylammonium pentafluorobenzenesulfonate
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
In 100 ml of methanol, 25 g of pentafluorobenzenesulfonyl chloride was dissolved under ice cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto. Stirring at room temperature for 3 hours provided a solution of tetramethylammonium pentafluorobenzenesulfonate. This solution was used for salt exchange with a sulfonium salt and an iodonium salt.