Reaktion #1471658

Reaktionsgleichung

[2-(2-thienyl)ethylamino](2-chlorophenyl)acetamide

hydrogen bromide

→

[2-(2-thienyl)ethylamino](2-chlorophenyl)acetamide hydrobromide

Lösungsmittel

acetone

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISSOLUTIONis dissolve
2. 2
   Filtrationthe precipitated white crystals are filtered off
3. 3
   Waschenwashed with acetone
4. 4
   Sonstigedried

Vorschrift

14.7 g (0.05 mol) of [2-(2-thienyl)ethylamino](2-chlorophenyl)acetamide, prepared as described in Example 7, is dissolve din 150 ml of acetone. To the solution 4 ml of 60% aqueous hydrogen bromide solution is added and the precipitated white crystals are filtered off, washed with acetone and dried.

Quelle