Reaktion #1464564

Reaktionsgleichung

2-methylbenzoxazole

n-octyl iodide

→

3-n-octyl-2-methylbenzoxazolium iodide

Ausbeute 73.2%

Lösungsmittel

ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturat reflux for 18 h
2. 2
   TemperaturAfter cooling
3. 3
   Filtrationfiltered
4. 4
   Waschenwashed with ether
5. 5
   Sonstigedried

Vorschrift

A stirred solution of 2-methylbenzoxazole (10.0 g, 75 mmol) and n-octyl iodide (18.0 g, 75 mmol) was heated at reflux for 18 h. After cooling, the yellow-brown solid was slurried in ether, filtered and washed with ether. The resulting solid was air dried to give (20.5 g, 73%) of 3-n-octyl-2-methylbenzoxazolium iodide.

Quelle