Reaktion #1463755

ord-2a650674cf404df5a59611107ab27189

Reaktionsgleichung

CCCCCCS(=O)(=O)O
hexane-1-sulphonic acid
CC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCN
desferrioxamine-B
→
CCCCCCS(=O)(=O)[O-]
hexane-1-sulphonate
CC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCN
desferrioxamine-B

Edukte

CCCCCCS(=O)(=O)O
hexane-1-sulphonic acid
CC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCN
desferrioxamine-B

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeare reacted

Vorschrift

Following a procedure analogous to that of Example 1, hexane-1-sulphonic acid and desferrioxamine-B are reacted to give the hexane-1-sulphonate salt of desferrioxamine-B. Mp 138° C. C31H62O11N6S Calcd C: 51.22%, H: 8.60%, N: 11.56%, S: 4.41%; Found C: 51.04%, H: 8.50%, N: 11.40%, S: 4.19%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05663201uspto-grants-1997_09