Reaktion #1457787

ord-2c7839d733b142d0881695e96db12e4f

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe reaction was quenched with hydrochloric acid
  2. 2
    Sonstigethe mixture was purified as usual,

Vorschrift

A Grignard reagent was prepared from 1-bromonaphthalene and magnesium in diethyl ether under an inert atmosphere. The reagent was reacted with 9-anthrone. The reaction was quenched with hydrochloric acid, and the mixture was purified as usual, to give the desired 9-α-naphthylanthracene.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06582837B1uspto-grants-2003_06