Reaktion #1447117
ord-3ddd7d4e011440eb9d7c77cc15a78b39
Reaktionsgleichung
4-chlorophenyl dichlorophosphate
L-alanine ethyl ester hydrochloride
Et3N
→
title compound
Ethyl N-[chloro(4-chlorophenoxy)phosphoryl]-L-alaninate
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
Following the procedure described for Example 1, step 2, treatment of a solution in DCM (0.090 M) of 4-chlorophenyl dichlorophosphate with L-alanine ethyl ester hydrochloride (1.0 eq.) and Et3N (2.0 eq.) provided the title compound as a colorless oil as a 1:1* mixture of diastereoisomers.