Reaktion #1437719

ord-f7595f8d7cf949c4a50826b082165e21

Reaktionsgleichung

CCC=C(CCC)c1c2cccc(-c3c(C)cc(C)cc3C)c2nn1C.Cl
2-Methyl-3-(1-propyl-but-1-enyl)-7-(2,4,6-trimethyl-phenyl)-2H-indazole Hydrochloride
CCCC(O)(CCC)c1c2cccc(-c3c(C)cc(C)cc3C)c2nn1C
4-[2-Methyl-7-(2,4,6-trimethyl-phenyl)-2H-indazol-3-yl]-heptan-4-ol
→
Cc1cc(C)c(-c2cccc3cn(C)nc23)c(C)c1
2-Methyl-7-(2,4,6-trimethyl-phenyl)-2H-indazole

Edukte

CCC=C(CCC)c1c2cccc(-c3c(C)cc(C)cc3C)c2nn1C.Cl
2-Methyl-3-(1-propyl-but-1-enyl)-7-(2,4,6-trimethyl-phenyl)-2H-indazole Hydrochloride
—
6b
CCCC(O)(CCC)c1c2cccc(-c3c(C)cc(C)cc3C)c2nn1C
4-[2-Methyl-7-(2,4,6-trimethyl-phenyl)-2H-indazol-3-yl]-heptan-4-ol

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

2-Methyl-3-(1-propyl-but-1-enyl)-7-(2,4,6-trimethyl-phenyl)-2H-indazole Hydrochloride (Ib or 6b Scheme 1)—Prepared from 4-[2-Methyl-7-(2,4,6-trimethyl-phenyl)-2H-indazol-3-yl]-heptan-4-ol (5b) using the procedure in step 8 of Example 1.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07214699B2uspto-grants-2007_05