Reaktion #1436626

Reaktionsgleichung

sodium hydroxide

Lithium aluminum hydride

2′-methoxyacetophenone

water

water

→

title compound

1-(2-Methoxyphenyl)ethanol

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturcooling
2. 2
   TrocknenThe organic layer was dried over magnesium sulfate
3. 3
   Einengenconcentrated under reduced pressure

Vorschrift

Lithium aluminum hydride (1.52 g) was suspended in tetrahydrofuran (100 ml), 2′-methoxyacetophenone (2.76 ml) was added under ice-cooling, and the mixture was stirred for 30 min. To the reaction mixture were successively added water (1.5 ml), 15% aqueous sodium hydroxide solution (1.5 ml) and water (4.5 ml). The organic layer was dried over magnesium sulfate and concentrated under reduced pressure to give the title compound (3.05 g).

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